PILOEX 250-SR, Pharmaceuticals and cosmetics

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PILOEX 250-SR

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This mixer-settler apparatus has been designed to study liquid-liquid-extraction processes. One part of the component, which has to be separated from the liquid phase (raffinate phase) is extracted by means of a liquid solvent (extract phase). This component is concentrated in the solvent (extract phase from the extraction phase to extraction phase). The raffinate phase and the extract phase will be led through the system in opposite directions. The advantage of the mixer-settler apparatus is the high efficiency of the exchange stages.
The latest re-design of EMS 250 SR liquid-liquid extractor consists of a 10-stage Mixer-Settler arrangement to work simultaneously.
Each stage consists of a mixer with downstream settler. In the mixer the light and the heavy phase from the neighbouring stages are brought together, are intensively mixed and then simultaneously conveyed into the settler. The mixing is realized by motor driven spiral stirrers for each mixing stage. Due to the intensive mixing the phases are divided into drops, so that the greater exchange surface, the substance transfer from one phase to another is heavily intensified.
Together with the component to be extracted, e.g. heavy phase, the raffinate phase is pumped from the raffinate store into the mixer of the last stage of the extractor. The solvent, e.g. light phase is pumped from the corresponding store tank into the mixer of the first stage of the extractor. Both phases, raffinate and extract are led into opposite directions through the extractor, the raffinate phase from the last stage and the extract phase from the first to the last extraction stage.
On it’s way through the apparatus the component which is to be extracted, is increasingly separated from stage to stage. Simultaneously the solvent stream (extract phase) absorbes more and more of the extracted component. The raffinate phase from which the component has been extracted, leaves the extractor at the first stage and is collected in a collecting vessel. The extracted phase leaded with the extracted component leaves the extractor at the last stage and is collected in a collecting vessel.
Contrary to other separation methods, the extraction will not directly lead to pure components. The extract phase is e.g. to be separated in a downstream distillation/rectification into extracted component and solvent.
This extraction process has the advantage of a low energy consumption for the separation of various compounds of liquid mixtures and is ideally applicable for demonstration purposes as well as for studying liquid-liquid extraction fundamentals in research and education.

Applications
• metal salt extractions
• liquids with low surface tension
• difficult coalescence in dispersed phase
• variation of the resident time for phases in the extraction stages
• reactions occuring during the extraction procedure
• considerable variations of the density during extraction