Domed Cooling Stage for Four-Circle Goniometers
• For in-situ X-ray diffraction studies at low and high temperatures on four-circle goniometers and XYZ stages
• Temperature range from -180 °C to +500 °C
• For the investigation of layered structures, phase transformations, and stress in crystalline material
The DCS 500 Domed Cooling Stage is the smallest attachment for in-situ X-ray diffraction studies at low and high temperatures on four-circle goniometers and XYZ stages. With a temperature range from -180 °C to +500 °C and a theta angle from almost 0° to 90° 2Θ for all Φangles, DCS 500 is the ideal sample stage for in-situ studies of layered structures and for investigating phase transformations and stress in crystalline material.
Exact sample temperature and variable sample environment
• Liquid nitrogen cryostat for fast cooling down to -180 °C
• Resistance heater for fast heating up to +500 °C
• Accurate PT100 RTD close to the sample for precise temperature measurement and control
• Highly X-ray transparent graphite dome for measurements under vacuum, in air and other gases
Compact design
• Smart and variable sample fixing allows reflectivity measurements
• Low weight (850 g)
• Thin, vacuum-insulated liquid nitrogen hoses with high flexibility down to -180 °C
| Model | DCS 500 |
| | |
| in air, inert gas | 25 °C to 500 °C |
| In vacuum (< 5x10-1 mbar) | -180 °C to 500 °C |
| Temperature measurement | PT100 |
| Atmospheres | Vacuum (10-1 mbar), air, inert gas |
| Max. operating pressure | 0.3 bar above atmospheric pressure |
| Sample holder material | Nickel-plated copper alloy |
| Sample diameter | max. 25 mm |
| Dome material | Graphite |
| Transmission | Cu Kα 72 % |
| Measuring geometry | Reflection |
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Платформи для рентгенівської дифракції.pdf
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